71.080.60 (Alcohols. Ethers) 标准查询与下载



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These test methods measure certain chemical and physical properties of ethylene glycols and propylene glycols and may be used to determine compliance with specification in which limits are established for these properties. For those tests that use the procedure of another ASTM test method, that test method should be consulted for additional information on the significance and use of that test. Alternative test methods and technology for several of the methods can be found in the Appendix. Use of these methods is optional and individuals using the alternative methods should assure themselves that the method is sufficient and appropriate for the application. Precision data presented in this standard is only for the original test methods listed.1.1 These test methods cover the chemical and physical analysis of the commonly available grades of ethylene glycol, diethylene glycol, triethylene glycol, propylene glycol, and dipropylene glycol. The key sections appear in the following order: Sections Purity of Reagents 4 Specific Gravity 6-8 Distillation Range 9-11 Acidity12-14 Water15-17 Iron18-20 Color21-23 Gas Chromatographic Analysis24-26 Alternative Test MethodsAppendix X1 1.2 Review the current appropriate Material Safety Data Sheets (MSDS) for detailed information concerning toxicity, first aid procedures, and safety precautions. 1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard with the exception of foot-pound for apparatus descriptions. 1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

Standard Test Methods for Analysis of Ethylene Glycols and Propylene Glycols

ICS
71.080.60 (Alcohols. Ethers)
CCS
发布
2012
实施

1.1 This specification covers n-butyl alcohol (butanol). 1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. 1.3 The following applies to all specified limits in this standard; for purposes of determining conformance with this standard, an observed value or a calculated value shall be rounded off “to the nearest unit” in the last right-hand digit used in expressing the specification limit, in accordance with the rounding-off method of Practice E29. 1.4 For hazard information and guidance, see the supplier's Material Safety Data Sheets.

Standard Specification for n-Butyl Alcohol (Butanol)

ICS
71.080.60 (Alcohols. Ethers)
CCS
G17
发布
2011
实施

1.1 This specification covers isobutyl alcohol for use in paint, varnish, lacquer, and related products. 1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. 1.3 The following applies to all specified limits in this standard; for purposes of determining conformance with this standard, an observed value or a calculated value shall be rounded off “to the nearest unit” in the last right-hand digit used in expressing the specification limit, in accordance with the rounding-off method of Practice E29. 1.4 For specific hazard information and guidance, see the supplier's Material Safety Data Sheets for materials listed in this specification.

Standard Specification for Isobutyl Alcoholl

ICS
71.080.60 (Alcohols. Ethers)
CCS
G17
发布
2011
实施

1.1 This specification covers 2-ethoxyethanol.1.2 The values stated in SI units are to be regarded as the standard. No other units of measurement are included in this standard.1.3 The following applies to all specified limits in this standard; for purposes of determining conformance with this standard, an observed value or a calculated value shall be rounded off "to the nearest unit" in the last right-hand digit used in expressing the specification limit, in accordance with the rounding-off method of Practice E 29.1.4 For hazard information and guidance, see the supplier's Material Safety Data Sheets.

Standard Specification for 2-Ethoxyethanol

ICS
71.080.60 (Alcohols. Ethers)
CCS
G17
发布
2011
实施

1.1 This specification covers n-propyl alcohol (1-propanol) for use in paint, varnish, lacquer and related products. 1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. 1.3 The following applies to all specified limits in this standard; for purposes of determining conformance with this standard, an observed value or a calculated value shall be rounded off “to the nearest unit” in the last right-hand digit used in expressing the specification limit, in accordance with the rounding-off method of Practice E29. 1.4 For specific hazard information and guidance, see the supplier's Material Safety Data Sheets for materials listed in this specification.

Standard Specification for 1-Propanol (n-Propyl Alcohol)

ICS
71.080.60 (Alcohols. Ethers)
CCS
G17
发布
2011
实施

4.1 Any residual fatty acid and esters (FA&E) should be present only at very low levels in purified glycerine. 4.2 This procedure requires the addition of a measured volume of sodium hydroxide, in excess of the amount actually needed to react with FA&E in the glycerine sample. After boiling, the excess sodium hydroxide is back titrated with standardized hydrochloric acid. The quantity of the substance being titrated is calculated as the difference between the volumes of the sodium hydroxide solution originally added, corrected by means of a blank titration, and that was consumed by the titrant in the back titration. Note 1: The standardized solutions for sodium hydroxide and hydrochloric acid are commercially available. 1.1 This test method provides the quantitative determination of the fatty acid and ester content in purified glycerin by the titrimetric method. 1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. 1.3 This standard may involve hazardous materials, operations and equipment. This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Specific precautions are listed in Section 8.

Standard Test Method for Determination of Fatty Acids and Esters in Glycerin

ICS
71.080.60 (Alcohols. Ethers)
CCS
发布
2010
实施

4.1 This test method is based on the cold oxidation of the glycerol by sodium metaperiodate in a strong acidic medium. Formaldehyde and formic acid are produced in this reaction and the latter is used to measure the glycerol content by titration with standard sodium hydroxide solution, to a pH 8.1 ± 0.1. The glycerol content is expressed as a percentage (m/m). 4.2 Interferences—The glycerin sample should be free of organic compounds with more than two hydroxyl groups on adjacent carbon atoms (for example, sugars, glycols). These types of compounds may produce formic acid which interferes with the determination of the glycerol content. 1.1 This test method provides the quantitative determination of glycerin by the titrimetric method. It is applicable to all glycerin or glycerin/water mixtures >758201;%. 1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. 1.3 This standard may involve hazardous materials, operations and equipment. This standard does not purport to address all of the safety problems associated with its use. It is the responsibility of whoever uses this standard to consult the established and appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Specific precautions are listed in Section 8.

Standard Test Method for Determination of Glycerin Assay by Titration (Sodium Meta Periodate)

ICS
71.080.60 (Alcohols. Ethers)
CCS
发布
2010
实施

1.1 This specification covers dipropylene glycol monomethyl ether (DPM). Note 18212;Dipropylene glycol monomethyl ether (DPM) is a mixture of isomers, the predominant isomer being 1-(2-methoxy-1-methylethoxy)-2-propanol. 1.2 The following applies to all specified limits in this standard; for purposes of determining conformance with this standard, an observed value or a calculated value shall be rounded off “to the nearest unit” in the last right-hand digit used in expressing the specification limit, in accordance with the rounding-off method of Practice E 29. 1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. 1.4 For specific hazard information and guidance, consult the supplier's Material Safety Data Sheet for materials listed in this standard.

Standard Specification for Dipropylene Glycol Monomethyl Ether

ICS
71.080.60 (Alcohols. Ethers)
CCS
G17
发布
2009-01-01
实施

1.1 This specification covers industrial grade ethylene glycol. 1.2 Review the current Materials Safety Data Sheets (MSDS) for detailed information concerning toxicity, first aid procedures, handling and safety precautions. 1.3 The following applies to all specified limits in this standard; for purposes of determining conformance with this standard, an observed value or a calculated value shall be rounded off “to the nearest unit” in the last right-hand digit used in expressing the specification limit, in accordance with the rounding-off method of Practice E29. 1.4 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. 1.5 The following safety hazards caveat pertains only to the test methods portion, Section 5, of this specification: This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

Standard Specification for Industrial Grade Ethylene Glycol

ICS
71.080.60 (Alcohols. Ethers)
CCS
发布
2009
实施

These test methods measure certain chemical and physical properties of ethylene glycols and propylene glycols and may be used to determine compliance with specification in which limits are established for these properties. For those tests that use the procedure of another ASTM test method, that test method should be consulted for additional information on the significance and use of that test. Alternative test methods and technology for several of the methods can be found in the Appendix. Use of these methods is optional and individuals using the alternative methods should assure themselves that the method is sufficient and appropriate for the application. Precision data presented in this standard is only for the original test methods listed.1.1 These test methods cover the chemical and physical analysis of the commonly available grades of ethylene glycol, diethylene glycol, triethylene glycol, propylene glycol, and dipropylene glycol. The key sections appear in the following order: Sections Purity of Reagents 4 Specific Gravity 6-8 Distillation Range 9-11 Acidity12-14 Water15-17 Iron18-20 Color21-23 Gas Chromatographic Analysis24-26 Alternative Test MethodsAppendix X1 1.2 Review the current appropriate Material Safety Data Sheets (MSDS) for detailed information concerning toxicity, first aid procedures, and safety precautions. 1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

Standard Test Methods for Analysis of Ethylene Glycols and Propylene Glycols

ICS
71.080.60 (Alcohols. Ethers)
CCS
发布
2009
实施

This test method provides for the quantitative determination of total acidity in ethylene glycols by non-aqueous potentiometric titration. The run time for titration of ethylene glycol samples ranges from 5 to 10 min with no sample preparation required. The length of time for a titration depends on the amount of acidity in the sample and the acidity generally increases from monoethylene glycol to the higher glycols like tetraethylene glycol. Acceptable levels of acidity in ethylene glycols vary with the manufacturer’s specifications but are normally below 200 mg/kg. Knowledge of the acidity in ethylene glycols is required to establish whether the product quality meets specification requirements.1.1 This test method covers the determination of total acidity as acetic acid in commonly available grades of monoethylene glycol, diethylene glycol, triethylene glycol and tetraethylene glycol using a non-aqueous potentiometric titration. This test method is useful for determining low levels of acidity, below 200 mg/kg. 1.2 The mono-, di-, tri- and tetraethylene glycols can be analyzed directly by this test method without any sample preparation. 1.3 Review the current appropriate Material Safety Data Sheets (MSDS) for detailed information concerning toxicity, first aid procedures, and safety precautions. 1.4 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. 1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Specific hazards statements are given in the section on Hazards, Section 9.

Standard Test Method for Acidity in Mono-, Di-, Tri- and Tetraethylene Glycol by
Non-Aqueous Potentiometric Titration

ICS
71.080.60 (Alcohols. Ethers)
CCS
G16
发布
2009
实施

1.1 This specification covers industrial grade ethylene glycol. 1.2 The following safety hazards caveat pertains only to the test method portion, Section 5, of this specification: This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. 1.3 Review the current Materials Safety Data Sheets (MSDS) for detailed information concerning toxicity, first aid procedures, handling and safety precautions. 1.4 The following applies to all specified limits in this standard; for purposes of determining conformance with this standard, an observed value or a calculated value shall be rounded off “to the nearest unit” in the last right-hand digit used in expressing the specification limit, in accordance with the rounding-off method of Practice E29. 1.5 The values stated in SI units are to be regarded as the standard.

Standard Specification for Industrial Grade Ethylene Glycol

ICS
71.080.60 (Alcohols. Ethers)
CCS
G16
发布
2009
实施

These test methods are suitable for manufacturing control and for determining compliance with specification limits for the properties designated by the test methods. For those test methods that use the procedure given in other ASTM methods, those test methods should be consulted for additional information on the significance, use, and possible interferences.1.1 These test methods cover chemical and physical tests for measuring the quality of methanol and appear in the following order: Sections Purity of Reagents4 Safety Precautions5 Sampling6 Acidity7 to 9 Carbonizables10 to 18 Color19 to 21 Distillation Range22 to 24 Permanganate Time25 to 27 Specific Gravity28 to 30 Water31 to 33 Water Miscibility34 to 37 Ethanol37 to 47 Acetone48 to 55 Trimethylamine56 to 65 1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. 1.3 Review the current Material Safety Data Sheets (MSDS) for detailed information concerning toxicity, first aid procedures and safety precautions for the chemicals used in this standard. 1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Specific hazards statements are given in Sections 5 and 15 and in 16.1, 16.4, and 52.2.2. 10.1 This test method describes a procedure for detecting the presence of impurities in methanol that carbonize or darken in the presence of concentrated sulfuric acid. The test method is applicable to methanol having a carbonizables content in the range from 0 to 70 on the platinum-cobalt scale (see Test Method D 1209). 37.1 This test method is applicable to methanol in which the ethanol content is between 0 and 1000 μg/g. 48.1 This test method covers a procedure for detecting the presence of acetone in methyl alcohol (methanol) in amounts greater than 0.003 weight % mass (m/m) . 56.1 This test method is used to determine the trimethylamine (TMA) content of refined methanol in the range of 10 to 100 μg/kg. 56.2 The odor of methanol has been determined to be caused primarily by the impurity TMA. The determination of TMA and its......

Standard Test Method for Analysis of Methanol

ICS
71.080.60 (Alcohols. Ethers)
CCS
G16
发布
2008
实施

3.1 These test methods are suitable for manufacturing control and for determining compliance with specification limits for the properties designated by the test methods. For those test methods that use the procedure given in other ASTM methods, those test methods should be consulted for additional information on the significance, use, and possible interferences. 1.1 These test methods cover chemical and physical tests for measuring the quality of methanol and appear in the following order:   Sections Purity of Reagents 4 Safety Precautions 5 Sampling 6 Acidity 7 to 9 Carbonizables 10 to 18 Color 19 to 21 Distillation Range 22 to 24 Permanganate Time 25 to 27 Specific Gravity 28 to 30 Water 31 to 33 Water Miscibility 34 to 37 Ethanol 37 to 47 Acetone 48 to 55 Trimethylamine 56 to 65 1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

Standard Test Methods for Analysis of Methanol

ICS
71.080.60 (Alcohols. Ethers)
CCS
发布
2008
实施

1.1 This specification covers engine coolant grade 1,3-propanediol (PDO). 1.2 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only. 1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

Standard Specification for Engine Coolant Grade 1,3-Propanediol (PDO)

ICS
71.080.60 (Alcohols. Ethers)
CCS
G17
发布
2008
实施

1.1 This specification covers propylene glycol monomethyl ether acetate (PMA). Note 1???Propylene glycol monomethyl ether acetate (PMA) is a mixture of 1-methoxy-2-acetoxypropane and 2-methoxy-1-acetoxypropane. 1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. 1.3 The following applies to all specified limits in this standard; for purposes of determining conformance with this standard, an observed value or a calculated value shall be rounded off ???to the nearest unit??? in the last right-hand digit used in expressing the specification limit, in accordance with the rounding-off method of Practice E29. 1.4 For specific hazard information and guidance, consult the supplier's Material Safety Data Sheet for materials listed in this standard.

Standard Specification for Propylene Glycol Monomethyl Ether Acetate

ICS
71.080.60 (Alcohols. Ethers)
CCS
G17
发布
2008
实施

1.1 This specification covers propylene glycol monomethyl ether acetate (PMA). Note 18212;Propylene glycol monomethyl ether acetate (PMA) is a mixture of 1-methoxy-2-acetoxypropane and 2-methoxy-1-acetoxypropane. 1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. 1.3 The following applies to all specified limits in this standard; for purposes of determining conformance with this standard, an observed value or a calculated value shall be rounded off “to the nearest unit” in the last right-hand digit used in expressing the specification limit, in accordance with the rounding-off method of Practice E 29. 1.4 For specific hazard information and guidance, consult the supplier's Material Safety Data Sheet for materials listed in this standard.

Standard Specification for Propylene Glycol Monomethyl Ether Acetate

ICS
71.080.60 (Alcohols. Ethers)
CCS
G17
发布
2008
实施

1.1 This specification covers engine coolant grade 1,3-propanediol (PDO). 1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. 1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

Standard Specification for Engine Coolant Grade 1,3-Propanediol lpar;PDOrpar;

ICS
71.080.60 (Alcohols. Ethers)
CCS
发布
2008
实施

1.1 This specification covers regular and monomer grade 2-ethylhexanol.1.2 The following applies to all specified limits in this standard; for purposes of determining conformance with this standard, an observed value or a calculated value shall be rounded off "to the nearest unit" in the last right-hand digit used in expressing the specification limit, in accordance with the rounding-off method of Practice E 29.1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.4 For specific hazard information and guidance, see the supplier's Material Safety Data Sheet for materials listed in this specification.

Standard Specification for 2-Ethylhexanol

ICS
71.080.60 (Alcohols. Ethers)
CCS
G16
发布
2007
实施

1.1 This specification covers propylene glycol monomethyl ether (PM). Note 1Propylene glycol monomethyl ether (PM) is a mixture of two isomers: 1-methoxy-2-propanol and 2-methoxy-1-propanol.1.2 The following applies to all specified limits in this standard; for purposes of determining conformance with this standard, an observed value or a calculated value shall be rounded off "to the nearest unit" in the last right-hand digit used in expressing the specification limit, in accordance with the rounding-off method of Practice E 29.1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.4 For specific hazard information and guidance, consult the supplier's Material Safety Data Sheet for materials listed in this standard.

Standard Specification for Propylene Glycol Monomethyl Ether

ICS
71.080.60 (Alcohols. Ethers)
CCS
G17
发布
2007
实施



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